4-苄氧基-3-甲氧基苯乙酮合成路线 （共 35 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=40°C;
参考文献
WO2005/30140 A2, ;
Page/Page column 198 ;
WO 2005/030140 A2
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 6 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 48, p. 371 - 378
反应条件
in pyridine T=5°C; 0.166667 h;
参考文献
Tetrahedron, , vol. 53, # 23 p. 7877 - 7888
反应条件
in methanol; diethyl ether 1 h; Ambient temperature;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 30, # 5 p. 1567 - 1573
反应条件
sulfuric acid Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 825 - 831
反应条件
1: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation 2: 99 percent / pyridine / 0.17 h / 5 °C View Scheme
参考文献
Tetrahedron, , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 2: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation 3: 99 percent / pyridine / 0.17 h / 5 °C View Scheme
参考文献
Tetrahedron, , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C 2: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h 3: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 4: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation 5: 99 percent / pyridine / 0.17 h / 5 °C View Scheme
参考文献
Tetrahedron, , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h 2: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 3: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation 4: 99 percent / pyridine / 0.17 h / 5 °C View Scheme
参考文献
Tetrahedron, , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 7 percent / phenylmethanol; dimethylsulfoxide / 0.03 h / 190 °C 2: 70 percent / methanol; diethyl ether / 1 h / Ambient temperature View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 30, # 5 p. 1567 - 1573
