溴代-3,4-二甲氧基苯乙酮合成路线 （共 30 条）
反应条件
bromine in chloroform 3 h; Heating;
参考文献
Moreno, Isabel; Tellitu, Imanol; Dominguez, Esther; SanMartin, Raul
European Journal of Organic Chemistry, 2002 , # 13 p. 2126 - 2135
反应条件
[BMIM(SO3H)][OTf]; N-bromosuccinmide T=55°C; 1 h; Green chemistry;
参考文献
Molecules, , vol. 18, # 1 p. 74 - 96
反应条件
aluminium trichloride in dichloromethane T=20°C; 12 h;
参考文献
Varache-Beranger; Nuhrich; Devaux
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 6 p. 465 - 473
反应条件
1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether / acetone / 4 h / 25 °C / |Inert atmosphere; |Green chemistry 2: bromine / chloroform / 4 h / 0 °C / |Reflux View Scheme
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 4 p. 781 - 787
反应条件
in diethylene glycol dimethyl ether T=160°C;
参考文献
Chemistry Letters, , p. 209 - 212
反应条件
1: AlCl3 2: Br2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 37, # 26 p. 4371 - 4376
反应条件
1: (i) LDA, THF, (ii) /BRN= 473899/ 2: bis-(2-methoxy-ethyl) ether / 160 °C View Scheme
参考文献
Chemistry Letters, , p. 209 - 212
反应条件
potassium carbonate in acetone
参考文献
Pardini, Vera L.; Smith, Carmen Z.; Utley, James H. P.; Vargas, Reinaldo R.; Viertler, Hans
Journal of Organic Chemistry, 1991 , vol. 56, # 26 p. 7305 - 7313
反应条件
1: sodium carbonate / N,N-dimethyl-formamide / 3 h / 25 °C 2: sodium tetrahydroborate / tetrahydrofuran; water / 0.33 h / |Reflux 3: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / |Green chemistry 4: 25 °C View Scheme
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
反应条件
1: sodium carbonate / N,N-dimethyl-formamide / 3 h / 25 °C 2: sodium tetrahydroborate / tetrahydrofuran; water / 0.33 h / |Reflux 3: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / |Green chemistry View Scheme
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
