2-(三甲基硅氧基)丙烯合成路线 （共 98 条）
反应条件
di-n-butylbis(trifluoromethanesulfonyloxy)stannane in dichloromethane
T=-50°C; 2 h;
参考文献
Sato, Tsuneo; Wakahara, Yoshiyuki; Otera, Junzo; Nozaki, Hitosi
Tetrahedron, 1991 , vol. 47, # 47 p. 9773 - 9782
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-78°C; Mukaiyama aldol reaction; Product distribution; Further Variations:Reaction partnersReagents;
参考文献
Shirakawa, Seiji; Maruoka, Keiji
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1469 - 1472
反应条件
ammonium cerium(IV) nitrate; sodium hydrogencarbonate in acetonitrile
0.0833333 h; Ambient temperature;
参考文献
Baciocchi, Enrico; Casu, Angela; Ruzziconi, Renzo
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3707 - 3710
反应条件
[Rh(1,5-cyclooctadiene)(PMePh2)2]OTf in dichloromethane
T=80°C; Substitution; 19 h; Title compound not separated from byproducts;
参考文献
Muraoka; Matsuda; Itoh
Tetrahedron Letters, 2000 , vol. 41, # 45 p. 8807 - 8811
反应条件
[Rh(1,5-cyclooctadiene)(PMePh2)2]OTf in dichloromethane
T=80°C; Substitution; 19 h; Title compound not separated from byproducts;
参考文献
Muraoka; Matsuda; Itoh
Tetrahedron Letters, 2000 , vol. 41, # 45 p. 8807 - 8811
反应条件
T=40°C; 40 h; Irradiation; Further byproducts given;
参考文献
Voronkov, M. G.; Rakhlin, V. I.; Khangazeev, S. Kh.; Mirskov, R. G.; Dneprovskii, A. S.
Doklady Chemistry, 1981 , vol. 259, p. 386 - 388
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 259, # 6 p. 1364 - 1366
反应条件
ammonium cerium(IV) nitrate; sodium hydrogencarbonate in acetonitrile
0.0833333 h; Ambient temperature;
参考文献
Baciocchi, Enrico; Casu, Angela; Ruzziconi, Renzo
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3707 - 3710
反应条件
[Rh(1,5-cyclooctadiene)(PMePh2)2]OTf in dichloromethane
T=80°C; Substitution; 19 h; Title compound not separated from byproducts;
参考文献
Muraoka; Matsuda; Itoh
Tetrahedron Letters, 2000 , vol. 41, # 45 p. 8807 - 8811
反应条件
bromine in dichloromethane
参考文献
Zembayashi,M. et al.
Synthesis, 1977 , p. 422 - 423
反应条件
pyridine; silver trifluoromethanesulfonate; trichloromethyl chloroformate
1) ether, 0 deg C, 15 min, 2) r.t., 2 h; Yield given. Multistep reaction;
参考文献
Takeda, Kazuyoshi; Ayabe, Akira; Kawashima, Hideki; Harigaya, Yoshihiro
Tetrahedron Letters, 1992 , vol. 33, # 7 p. 951 - 952
