2-(三甲基硅氧基)丙烯合成路线 （共 98 条）
反应条件
in dichloromethane
Heating;
参考文献
Hambly, G. F.; Chan, T. H.
Tetrahedron Letters, 1986 , vol. 27, # 23 p. 2563 - 2566
反应条件
sodium dithionite; sodium hydrogencarbonate in water; acetonitrile
T=40°C;
参考文献
Huang, Wei-yuan; Wu, Yong-ming
Journal of Fluorine Chemistry, 1992 , vol. 59, # 2 p. 179 - 183
反应条件
1: isopropenyloxy trimethylsilane With methyllithium in tetrahydrofuran
T=0°C; Metallation;
2: cyclohept-2-en-1-one With ATPH in tetrahydrofuran; toluene
T=-78°C; Michael addition; 0.3 h;
参考文献
Saito, Susumu; Shimada, Itsuro; Takamori, Yusuke; Tanaka, Michiaki; Maruoka, Keiji; Yamamoto, Hisashi
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 7 p. 1671 - 1681
反应条件
[Rh(I)(cycloocta-1,5-diene)(butane-1,4-diylbis[diphenylphosphine])]ClO4 in dichloromethane
T=100°C; 17 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izum, Yusuke
Tetrahedron Letters, 1987 , vol. 28, # 52 p. 6657 - 6660
反应条件
[Ir(cod)(PPh3)2]OTf; hydrogen in dichloromethane
T=25°C; crossed aldol coupling; desilylation; 3 h;
参考文献
Matsuda, Isamu; Hasegawa, Yuki; Makino, Tatsuya; Itoh, Kenji
Tetrahedron Letters, 2000 , vol. 41, # 9 p. 1405 - 1408
反应条件
N-chloro-succinimide in dichloromethane
Heating;
参考文献
Hambly, G. F.; Chan, T. H.
Tetrahedron Letters, 1986 , vol. 27, # 23 p. 2563 - 2566
反应条件
in dichloromethane
Heating;
参考文献
Hambly, G. F.; Chan, T. H.
Tetrahedron Letters, 1986 , vol. 27, # 23 p. 2563 - 2566
反应条件
zinc(II) iodide in diethyl ether
T=22°C; 2 h;
参考文献
Reetz, Manfred T.; Mueller-Starke, H.
Liebigs Annalen der Chemie, 1983 , # 10 p. 1726 - 1738
反应条件
pyridine in dichloromethane
1 h; Ambient temperature;
参考文献
Umemoto, Teruo; Kuriu, Yuriko; Nakayama, Shin-ichi; Miyano, Osamu
Tetrahedron Letters, 1982 , vol. 23, # 14 p. 1471 - 1474
反应条件
sodium dithionite; sodium hydrogencarbonate in water; acetonitrile
T=40°C;
参考文献
Huang, Wei-yuan; Wu, Yong-ming
Journal of Fluorine Chemistry, 1992 , vol. 59, # 2 p. 179 - 183
