2-(三甲基硅氧基)丙烯合成路线 （共 98 条）
反应条件
in dichloromethane
T=50°C; P=7500600 Torr; 168 h;
参考文献
Yamamoto, Yoshinori
Chemistry Letters, 1987 , p. 945 - 946
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris(dibenzylideneacetone)dipalladium (0); ZnF2 in N,N-dimethyl-formamide
T=150°C; 0.25 h; Irradiationmicrowave;
参考文献
Chobanian, Harry R.; Liu, Ping; Chioda, Marc D.; Guo, Yan; Lin, Linus S.
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1213 - 1216
反应条件
in 1,4-dioxane
Diels-Alder reaction; 18 h; Heating;
参考文献
Peng, Da-Quan; Liu, Yun; Lu, Zhi-Feng; Shen, Yong-Miao; Xu, Jian-Hua
Synthesis, 2008 , # 8 p. 1182 - 1192
反应条件
in 1,4-dioxane
Diels-Alder reaction; 18 h; Heating;
参考文献
Peng, Da-Quan; Liu, Yun; Lu, Zhi-Feng; Shen, Yong-Miao; Xu, Jian-Hua
Synthesis, 2008 , # 8 p. 1182 - 1192
反应条件
T=40°C; 40 h; Irradiation; Further byproducts given;
参考文献
Voronkov, M. G.; Rakhlin, V. I.; Khangazeev, S. Kh.; Mirskov, R. G.; Dneprovskii, A. S.
Doklady Chemistry, 1981 , vol. 259, p. 386 - 388
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 259, # 6 p. 1364 - 1366
反应条件
1: isopropenyloxy trimethylsilane With potassium fluoride; dibenzo-18-crown-6; nonafluoro-n-butanesulfonyl fluoride in tetrahydrofuran
T=25°C; 120 h;
2: acrylic acid methyl ester With palladium diacetate; triethylamine; lithium chloride in N,N-dimethyl-formamide
T=25°C; 27 h;
参考文献
Lyapkalo, Ilya M.; Webel, Matthias; Reissig, Hans-Ulrich
European Journal of Organic Chemistry, 2002 , # 21 p. 3646 - 3658
反应条件
Nafion-TMS in dichloromethane
T=-78 - 20°C; 20 h; Yield given;
参考文献
Haunert, Frank; Bolli, Martin H.; Hinzen, Berthold; Ley, Steven V.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 15 p. 2235 - 2237
反应条件
dodecacarbonyltetrarhodium(0) in benzene
T=100°C; 40 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
