(3-氧代-1,3-二氢-1-异苯并呋喃)-乙腈合成路线 (共 8 条)
反应条件
copper diacetate; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in xylene 10 h; Heating;
参考文献
Ueura, Kenji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2007 , vol. 72, # 14 p. 5362 - 5367
反应条件
pyridine; tetrabutyl-ammonium chloride; [(t-Bu)3PH]BF4; palladium diacetate in 1,4-dioxane T=150°C; Michael addition; 0.333333 h; microwave irradiation;
参考文献
Wu, Xiongyu; Nilsson, Peter; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 346 - 349
反应条件
2-mesityl-2,5,6,7-tetrahydropyrrolo[2,1-c][1,2,4]triazol-4-ium chloride; triethylamine in toluene T=80°C; 22 h;
参考文献
Youn, So Won; Song, Hyoung Sub; Park, Jong Hyub
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 15 p. 2388 - 2393
反应条件
hydrogenchloride; P2O5 in anhydrous xylene
参考文献
Allergan, Inc.
Patent: US2004/19098 A1, 2004 ;
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl-formamide Heating;
参考文献
Parker, Julie A.; Stanforth, Stephen P.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 5 p. 1587 - 1588
反应条件
{RuCl2(1-methyl-4-(1-methylethyl)benzene)}2; copper (II) acetate monohydrate in water T=80°C; 0.333333 h; Inert atmosphere; chemoselective reaction;
参考文献
Ackermann, Lutz; Pospech, Jola
Organic Letters, 2011 , vol. 13, # 16 p. 4153 - 4155
反应条件
1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / 125 °C / |Inert atmosphere 2: 2-mesityl-2,5,6,7-tetrahydropyrrolo[2,1-c][1,2,4]triazol-4-ium chloride; triethylamine / toluene / 22 h / 80 °C View Scheme
参考文献
Youn, So Won; Song, Hyoung Sub; Park, Jong Hyub
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 15 p. 2388 - 2393
反应条件
in 1,4-dioxane; hexane; chloroform
参考文献
Allergan, Inc.
Patent: US2004/19098 A1, 2004 ;