N-(叔丁氧羰基)对甲苯磺酰胺合成路线 （共 29 条）
反应条件
[TMGH][OAc] T=20°C; 0.5 h; Neat (no solvent);
参考文献
Nouria, Azita; Akbari, Jafar; Heydaric, Akbar; Nouri, Arezu
Letters in Organic Chemistry, 2011 , vol. 8, # 1 p. 38 - 42
反应条件
1: in dichloromethane T=0 - 20°C; 2: With 5-hydroxymethylbicyclo[2.2.1]hept-2-ene in dichloromethane T=0 - 20°C; 3: With [{1,3-bis(mesyl)imidazolidin-2-yl}RuCl2(PCy3)(=CHPh)] in dichloromethane Heating; Further stages.;
参考文献
Moore, Joel D; Harned, Andrew M; Henle, Julia; Flynn, Daniel L; Hanson, Paul R
Organic letters, 2002 , vol. 4, # 11 p. 1847 - 1849
反应条件
hydrogen; palladium dihydroxide in ethanol P=760.051 Torr;
参考文献
Johnson II, David C.; Widlanski, Theodore S.
Tetrahedron Letters, 2004 , vol. 45, # 46 p. 8483 - 8487
反应条件
1: 99 percent / DMAP / tetrahydrofuran / 20 °C 2: 96 percent / hydrogen / Pearlman's catalyst / ethanol / 760.05 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 46 p. 8483 - 8487
反应条件
1: 93 percent / hydrogen / Pearlman's catalyst / ethanol / 760.05 Torr 2: 99 percent / DMAP / tetrahydrofuran / 20 °C 3: 96 percent / hydrogen / Pearlman's catalyst / ethanol / 760.05 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 46 p. 8483 - 8487
反应条件
1: 31 percent / tetrahydrofuran / 20 °C 2: 99 percent / DMAP / tetrahydrofuran / 20 °C 3: 96 percent / hydrogen / Pearlman's catalyst / ethanol / 760.05 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 46 p. 8483 - 8487
反应条件
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Cooling 2: hydrogenchloride; water / ethyl acetate / 4 h / 50 °C View Scheme
参考文献
Ohno, Hiroaki; Yamamoto, Mio; Iuchi, Mutsumi; Fujii, Nobutaka; Tanaka, Tetsuaki
Synthesis, 2011 , # 16 art. no. C50911SS, p. 2567 - 2578
反应条件
potassium hexamethylsilazane 1.) THF, -78 deg C, 2.) -78 deg C, 10 min, then to -50 deg C, 1.75 h; Yield given. Multistep reaction;
参考文献
Genet, Jean-Pierre; Hajicek, Josef; Bischoff, Laurent; Greck, Christine
Tetrahedron Letters, 1992 , vol. 33, # 19 p. 2677 - 2680
反应条件
trifluoroacetic acid T=0°C; 0.5 h;
参考文献
Johnson II, David C.; Widlanski, Theodore S.
Tetrahedron Letters, 2004 , vol. 45, # 46 p. 8483 - 8487
反应条件
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / |Inert atmosphere 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 4 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Nayak, Sanatan; Ghosh, Nayan; Sahoo, Akhila K.
Organic Letters, 2014 , vol. 16, # 11 p. 2996 - 2999
