7,8,15,16-四氧杂二螺(5.2.5.2)十六烷合成路线 （共 49 条）
反应条件
antimony(V) pentachloride in dichloromethane T=20°C; 0.75 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1950 - 1954
反应条件
hexafluoroisopropyl alcohol; toluene-4-sulfonic acid T=60°C; 0.5 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 82, # 7 p. 891 - 895
反应条件
in benzene T=140°C; other temperatures; ΔH(excit.), ΔS(excit.); Rate constantProduct distributionMechanism;
参考文献
Cafferata; Eyler; Svartman; Canizo; Bor kowski
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1058 - 1061
反应条件
antimony(V) pentachloride in dichloromethane T=20°C; 0.75 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1950 - 1954
反应条件
toluene-4-sulfonic acid in water
参考文献
Berkessel, Albrecht; Andreae, Marc R. M.; Schmickler, Hans; Lex, Johann
Angewandte Chemie - International Edition, 2002 , vol. 41, # 23 p. 4481 - 4484
反应条件
in benzene T=140°C; other temperatures; ΔH(excit.), ΔS(excit.); Rate constantProduct distributionMechanism;
参考文献
Cafferata; Eyler; Svartman; Canizo; Bor kowski
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1058 - 1061
反应条件
in benzene T=140°C; other temperatures; ΔH(excit.), ΔS(excit.); Rate constantProduct distributionMechanism;
参考文献
Cafferata; Eyler; Svartman; Canizo; Bor kowski
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1058 - 1061
反应条件
bismuth trifluoromethanesulphonate in dichloromethane; acetonitrile
T=20°C; 0.25 h;
参考文献
Sashidhara, Koneni V.; Avula, Srinivasa Rao; Ravithej Singh; Palnati, Gopala Reddy
Tetrahedron Letters, 2012 , vol. 53, # 36 p. 4880 - 4884
反应条件
dihydrogen peroxide in hexafluoroisopropyl alcohol; water
T=50°C; Baeyer-Villiger oxidation; 1.5 h;
参考文献
Piscopo, Calogero G.; Loebbecke, Stefan; Maggi, Raimondo; Sartori, Giovanni
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1625 - 1629
反应条件
bis(trimethylsilyl)-peroxide; trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=0°C; 1.5 h;
参考文献
Jefford, Charles W.; Boukouvalas, Amer Jaber John
Synthesis, 1988 , # 5 p. 391 - 393
