1: With oxygen; ozone in dichloromethane T=-78°C; 0.583333 h; 2: With dimethylsulfide in dichloromethane T=-78 - 20°C; 4 h; 3: With water; potassium carbonate in methanol T=55°C; 1 h;
参考文献
Magnin, David R.; Sulsky, Richard B.; Robl, Jeffrey A.; Caulfield, Thomas J.; Parker, Rex A.
Patent: US2003/225091 A1, 2003 ;
Location in patent: Page 29 ;
N-bromosuccinmide; diisopropylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Aitken, Harry R. M.; Furkert, Daniel P.; Hubert, Jonathan G.; Wood, James M.; Brimble, Margaret A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 31 p. 5147 - 5155
