N-methoxycarbonyl hydrazine in toluene
Michaelis-Arbuzov Synthesis; 2 h; Dean-StarkReflux;
参考文献
Debrouwer, Wouter; Heugebaert, Thomas S. A.; Van Hecke, Kristof; Stevens, Christian V.
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8232 - 8241
1: Et3N / toluene / 1 h / Ambient temperature
2: MgCl2 / toluene / 6 h / Ambient temperature
View Scheme
参考文献
Kim, Dae Young; Kong, Myeon Sik; Lee, Kilsung
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1997 , # 9 p. 1360 - 1364
magnesium chloride in toluene
6 h; Ambient temperature; Yield given;
参考文献
Kim, Dae Young; Kong, Myeon Sik; Lee, Kilsung
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1997 , # 9 p. 1360 - 1364