1-甲氧基-2-(3-甲基-3-丁烯-1-基)苯合成路线 （共 9 条）
反应条件
toluene-4-sulfonic acid in toluene Heating; Yields of byproduct given;
参考文献
Tsukayama, Masao; Kikuchi, Makoto; Kawamura, Yasuhiko
Heterocycles, 1994 , vol. 38, # 7 p. 1487 - 1490
反应条件
dilithium tetrachlorocuprate; magnesium in tetrahydrofuran; diethyl ether 1 h; Heating;
参考文献
Skatteboel, Lars; Nilsen, Nils O.; Myhren, Finn
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 10 p. 782 - 790
反应条件
1: 97 percent / PPh3, Et3N, PdCl2, CuI / dimethylformamide / 0.5 h / 50 °C 2: H2 / Raney Ni / methanol / 20 °C 3: TsOH*H2O / toluene / Heating View Scheme
参考文献
Heterocycles, , vol. 38, # 7 p. 1487 - 1490
反应条件
1: H2 / Raney Ni / methanol / 20 °C 2: TsOH*H2O / toluene / Heating View Scheme
参考文献
Heterocycles, , vol. 38, # 7 p. 1487 - 1490
反应条件
1: I2, CF3CO2Ag / CHCl3 / Ambient temperature 2: 97 percent / PPh3, Et3N, PdCl2, CuI / dimethylformamide / 0.5 h / 50 °C 3: H2 / Raney Ni / methanol / 20 °C 4: TsOH*H2O / toluene / Heating View Scheme
参考文献
Heterocycles, , vol. 38, # 7 p. 1487 - 1490
反应条件
1: 70 percent / pyridine, SOCl2 / benzene / 2.5 h / Heating 2: 1.) Mg turnings, iodine / 1.) ether, reflux, 30 min; 2.) ether, reflux, 1 h View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 66, p. 1 - 10
反应条件
1: 80 percent / NaBH4, 5percent NaOH / methanol; H2O / 12 h 2: 70 percent / pyridine, SOCl2 / benzene / 2.5 h / Heating 3: 1.) Mg turnings, iodine / 1.) ether, reflux, 30 min; 2.) ether, reflux, 1 h View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 66, p. 1 - 10
反应条件
1: methoxybenzene With 3,4,5,6-tetrachloro-1,2-benzoquinone; [CpMoCl(CO)3] T=20°C; Friedel Crafts-type alkylation; 0.5 h; Inert atmosphere; 2: 3,3-dimethylallyl alcohol T=60°C; Friedel Crafts-type alkylation; 6 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 14, # 34 p. 10705 - 10715
反应条件
sodium hydride; ethanethiol in N,N-dimethyl-formamide
2 h; Heating;
参考文献
Yates, Peter; Macas, Tadas S.
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1 - 10
