(5alpha,17beta)-3,3-二氟-雄甾烷-17-醇乙酸酯合成路线 （共 3 条）
1164-91-6(10,13-二甲基-3-氧代-1,2,4,5,6,7,8,9,11,12,14,15,16,17-十四氢环戊烯并[a]菲-17-基)乙酸酯
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反应条件
(diethylamido)sulfur trifluoride T=80°C; 3.5 h;
参考文献
Liu; Carlson; Katzenellenbogen
Journal of Medicinal Chemistry, 1992 , vol. 35, # 11 p. 2113 - 2129
反应条件
iodine monofluoride in chloroform 0.5 h; Ambient temperature;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700
反应条件
1: 98.3 percent / pyridine / CH2Cl2 / 2 h / Ambient temperature 2: 91 percent / (diethylamido)sulfur trifluoride / 3.5 h / 80 °C View Scheme
参考文献
Liu; Carlson; Katzenellenbogen
Journal of Medicinal Chemistry, 1992 , vol. 35, # 11 p. 2113 - 2129
