1: 750 °C / 0 - 0.1 Torr
2: 80 percent / Et3N / CH2Cl2 / 3 h / 0 °C
View Scheme
参考文献
Aitken, R. Alan; Armstrong, Jill M.; Drysdale, Martin J.; Ross, Fiona C.; Ryan, Bruce M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1999 , # 5 p. 593 - 604
1: 30percent aq. H2O2 / acetic acid / 1.33 h / Ambient temperature
2: potassium permanganate / acetone; H2O / 1 h / Ambient temperature
4: 99 percent / lithium tert-butyl hydroperoxide / tetrahydrofuran; toluene / 0.5 h / -78 °C
5: 69 percent / lithium iodide / acetone / 1 h / Heating
6: 67 percent / magnesium iodide / diethyl ether / 288 h / Ambient temperature
View Scheme
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3091 - 3102
2: 99 percent / lithium tert-butyl hydroperoxide / tetrahydrofuran; toluene / 0.5 h / -78 °C
3: 69 percent / lithium iodide / acetone / 1 h / Heating
4: 67 percent / magnesium iodide / diethyl ether / 288 h / Ambient temperature
View Scheme
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3091 - 3102
1: 69 percent / lithium iodide / acetone / 1 h / Heating
2: 67 percent / magnesium iodide / diethyl ether / 288 h / Ambient temperature
View Scheme
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3091 - 3102
