甲基 alpha-D-呋喃木糖苷合成路线 （共 15 条）
反应条件
1: 8.53 g / toluene-p-sulfonic acid / 20 h / 20 °C 2: NaH / dimethylformamide View Scheme
参考文献
Desai; Gigg
Carbohydrate Research, 1996 , vol. 280, # 2 p. 209 - 221
反应条件
1: 1-O-methyl-α/β-D-ribofuranoside With sodium hydride in tetrahydrofuran; N,N-dimethyl-formamide; mineral oil T=20°C; 0.0833333 h; Inert atmosphere; 2: benzyl bromide in tetrahydrofuran; N,N-dimethyl-formamide; mineral oil T=0 - 20°C; Inert atmosphere; optical yield given as percent de;
参考文献
Lou, Chenguang; Xiao, Qiang; Brennan, Lavinia; Light, Mark E; Vergara-Irigaray, Nuria; Atkinson, Elizabeth M.; Holden-Dye, Lindy M.; Fox, Keith R.; Brown, Tom
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 17 p. 6389 - 6397
反应条件
H-Dowex resin in acetone
参考文献
Van Derpoorten, Kim; Migaud, Marie E.
Organic Letters, 2004 , vol. 6, # 20 p. 3461 - 3464
反应条件
toluene-4-sulfonic acid T=20°C; 20 h;
参考文献
Desai; Gigg
Carbohydrate Research, 1996 , vol. 280, # 2 p. 209 - 221
反应条件
sulfuric acid T=0 - 20°C;
参考文献
Gammon, David W.; Hunter, Roger; Wilson, Seanette
Tetrahedron Letters, 2002 , vol. 43, # 17 p. 3141 - 3144
反应条件
TiCl4 in methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; chloroform; water
参考文献
Takeda Chemical Industries, Ltd.
Patent: US4689404 A1, 1987 ;
反应条件
1: NaH 2: 75 percent / aq. HCl / H2O View Scheme
参考文献
Mandai, Tadakatsu; Okumoto, Hiroshi; Oshitari, Tetsuta; Nakanishi, Katsuyoshi; Mikuni, Katsuhiko; Hara, Ko-ji; Hara, Ko-zo; Iwatani, Wakao; Amano, Tetsuya; Nakamura, Kosho; Tsuchiya, Yoshinori
Heterocycles, 2001 , vol. 54, # 2 p. 561 - 566
反应条件
1: NaH 2: 75 percent / aq. HCl / H2O View Scheme
参考文献
Mandai, Tadakatsu; Okumoto, Hiroshi; Oshitari, Tetsuta; Nakanishi, Katsuyoshi; Mikuni, Katsuhiko; Hara, Ko-ji; Hara, Ko-zo; Iwatani, Wakao; Amano, Tetsuya; Nakamura, Kosho; Tsuchiya, Yoshinori
Heterocycles, 2001 , vol. 54, # 2 p. 561 - 566
反应条件
1: NaH 2: 75 percent / aq. HCl / H2O View Scheme
参考文献
Mandai, Tadakatsu; Okumoto, Hiroshi; Oshitari, Tetsuta; Nakanishi, Katsuyoshi; Mikuni, Katsuhiko; Hara, Ko-ji; Hara, Ko-zo; Iwatani, Wakao; Amano, Tetsuya; Nakamura, Kosho; Tsuchiya, Yoshinori
Heterocycles, 2001 , vol. 54, # 2 p. 561 - 566
反应条件
1: pyridine / CH2Cl2 / 1) 0-5 deg C, 4 h, 2) 4-5 deg C, 12 h 2: AcOH, conc. H2SO4 / 4 - 5 °C View Scheme
参考文献
Tolstikov, G. A.; Baltina, L. A.; Khalilov, L. M.; Spirikhin, L. V.; Sultanmuratova, V. R.; Murinov, Yu. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 6 p. 623 - 626
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 6 p. 794 - 797
