1: 2-monochloropropane With magnesium in tetrahydrofuran 1 h; Heating; 2: 4-methoxy-benzaldehyde in tetrahydrofuran T=20°C; 3 h;
参考文献
Sharma, Gangavaram V. M.; Reddy, Katta Laxmi; Lakshmi, P. Sree; Ravi; Kunwar, Ajit C.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3967 - 3969
1-(2-methoxyphenyl)-2-methylpropan-1-one; trimethylaluminum; tri-n-butyl-tin hydride 1.) toluene, from -78 deg C to -40 deg C, 10 min, 2.) toluene; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ooi; Uraguchi; Kagoshima; Maruoka
Journal of the American Chemical Society, 1998 , vol. 120, # 21 p. 5327 - 5328
4'-methoxyisobutyrophenone; trimethylaluminum; tri-n-butyl-tin hydride 1.) toluene, from -78 deg C to -40 deg C, 10 min, 2.) toluene; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ooi; Uraguchi; Kagoshima; Maruoka
Journal of the American Chemical Society, 1998 , vol. 120, # 21 p. 5327 - 5328
