7,8,15,16,23,24-六氧杂三螺(5.2.5.2.5.2)二十四烷合成路线 （共 21 条）
反应条件
in various solvent(s) T=180 - 200°C; 3 h; Mechanism;
参考文献
Starostin, E. K.; Aleksandrov, A. V.; Ignatenko, A. V.; Nikitin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 133 - 136
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 141 - 144
参考文献
Synthesis, , p. 275 - 276
反应条件
in various solvent(s) T=180 - 200°C; 3 h; Further byproducts given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 1 p. 133 - 136
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 141 - 144
反应条件
in various solvent(s) T=180 - 200°C; 3 h; Mechanism;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 1 p. 133 - 136
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 141 - 144
反应条件
in various solvent(s) T=180 - 200°C; 3 h; Further byproducts given;
参考文献
Starostin, E. K.; Aleksandrov, A. V.; Ignatenko, A. V.; Nikitin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 133 - 136
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 141 - 144
反应条件
in various solvent(s) T=180 - 200°C; 3 h; Mechanism;
参考文献
Starostin, E. K.; Aleksandrov, A. V.; Ignatenko, A. V.; Nikitin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 133 - 136
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 141 - 144
反应条件
1: in dichloromethane
T=0°C; 0.5 h;
2: With sulfuric acid; acetonitrile in dichloromethane
T=0 - 20°C; 24 h;
参考文献
Neupane, Chiranjeev Sharma; Awasthi, Satish Kumar
Tetrahedron Letters, 2012 , vol. 53, # 45 p. 6067 - 6070,4
反应条件
boron trifluoride diethyl etherate in diethyl ether
T=20 - 25°C; 5 h;
参考文献
Terent'ev, Alexander O.; Platonov, Maxim M.; Sonneveld, Eduard J.; Peschar, Rene; Chernyshev, Vladimir V.; Starikova, Zoya A.; Nikishin, Gennady I.
Journal of Organic Chemistry, 2007 , vol. 72, # 19 p. 7237 - 7243
反应条件
boron trifluoride diethyl etherate in diethyl ether
T=20 - 25°C; 4 h;
参考文献
Terent'ev, Alexander O.; Platonov, Maxim M.; Sonneveld, Eduard J.; Peschar, Rene; Chernyshev, Vladimir V.; Starikova, Zoya A.; Nikishin, Gennady I.
Journal of Organic Chemistry, 2007 , vol. 72, # 19 p. 7237 - 7243
反应条件
sulfuric acid; dihydrogen peroxide in methanol
T=20°C; 24 h;
参考文献
McCullough, Kevin J.; Morgan, Alistair R.; Nonhebel, Derek C.; Pauson, Peter L.; White, Graham J.
Journal of Chemical Research, Miniprint, 1980 , # 2 p. 601 - 628
