1,2-乙烷二酮,1-[4-(溴甲基)苯基]-2-苯基合成路线 （共 4 条）
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
参考文献
Chemische Berichte, , vol. 101, # 4 p. 1480 - 1484
反应条件
1: (i) Py, (ii) /BRN= 607293/, aq. NaOH, EtOH
2: aq. H2SO4 / diethyl ether
3: aq. KMnO4
View Scheme
参考文献
Krieg,B.; Manecke,G.
Chemische Berichte, 1968 , vol. 101, # 4 p. 1480 - 1484
反应条件
1: PS-DIEA / CH2Cl2 / 20 °C
2: AcOH / ethanol / 0.17 h / 160 °C / microwave irradiation
View Scheme
参考文献
Lindsley, Craig W.; Zhao, Zhijian; Leister, William H.; Robinson, Ronald G.; Barnett, Stanley F.; Defeo-Jones, Deborah; Jones, Raymond E.; Hartman, George D.; Huff, Joel R.; Huber, Hans E.; Duggan, Mark E.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 3 p. 761 - 764
反应条件
1: With PS-DIEA in dichloromethane
T=20°C;
2: With fluorous-tagged thiol
参考文献
Lindsley, Craig W.; Bogusky, Michael J.; Leister, William H.; McClain, Ray T.; Robinson, Ronald G.; Barnett, Stanley F.; Defeo-Jones, Deborah; Ross III, Charles W.; Hartman, George D.
Tetrahedron Letters, 2005 , vol. 46, # 16 p. 2779 - 2782
