反应条件
1: dichloromethane / 4 h
2: lithium aluminium tetrahydride / diethyl ether / 4 h / 0 °C
3: potassium carbonate / 1,4-dioxane / 7 h / 100 °C
4: hydrogenchloride / 1,4-dioxane; water / 24 h / 20 °C
5: sodium hydroxide / dichloromethane / 12 h / 25 °C / pH 7 - 8
View Scheme
参考文献
Zhang, Yongmin; Feng, Yujun; Wang, Jiyu; He, Shuai; Guo, Zanru; Chu, Zonglin; Dreiss, Cecile A.
Chemical Communications, 2013 , vol. 49, # 43 p. 4902 - 4904
