4-(2-氰基乙基)苯甲腈合成路线 （共 11 条）
反应条件
Pd-PEPPSI-IPr in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=50°C; Negishi Coupling Reaction; 12 h; Inert atmosphere;
参考文献
LUDWIG-MAXIMILIANS-UNIVERSITAeT MUeNCHEN; KNOCHEL, Paul; BERNHARDT, Sebastian; MANOLIKAKES, Georg
Patent: WO2012/85168 A1, 2012 ;
Location in patent: Page/Page column 30; 32 ;
反应条件
manganese; water; trifluoroacetic acid; Co(2,2'-bipyridine)Br2; lithium bromide in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Amatore, Muriel; Gosmini, Corinne; Perichon, Jacques
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 6130 - 6134
反应条件
naphthonitrile in acetonitrile T=20°C; working electrodes: 15 cm2 platinum grid, 27 cm2 mercury pool; reference electrode: saturated calomel electrode (-1.8 V/SCE); 0.1 M NBu4BF4, constant current (20mA/cm2);
参考文献
Chami, Zoubida; Gareil, Monique; Pinson, Jean; Saveant, Jean-Michel; Thiebault, Andre
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 586 - 595
反应条件
sodium hydrogen telluride; acetic acid in ethanol; benzene 24 h; Ambient temperature;
参考文献
Blay, Gonzalo; Cardona, Luz; Garcia, Begona; Lahoz, Luisa; Pedro, Jose R.
Tetrahedron, 1996 , vol. 52, # 25 p. 8611 - 8618
反应条件
NSC26899; [Ru(2,2′-bipyridine)3]2+ in pyridine; methanol 1.5 h; Irradiation;
参考文献
Pac, Chyongjin; Miyauchi, Yoji; Ishitani, Osamu; Ihama, Mikio; Yasuda, Masahide; Sakurai, Hiroshi
Journal of Organic Chemistry, 1984 , vol. 49, # 1 p. 26 - 34
反应条件
naphthonitrile in acetonitrile T=20°C; working electrodes: 15 cm2 platinum grid, 27 cm2 mercury pool; reference electrode: saturated calomel electrode (-1.8 V/SCE); 0.1 M NBu4BF4, constant current (20mA/cm2);
参考文献
Chami, Zoubida; Gareil, Monique; Pinson, Jean; Saveant, Jean-Michel; Thiebault, Andre
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 586 - 595
反应条件
nickel in ethylene glycol dimethyl ether T=85°C; 0.25 h;
参考文献
Inaba, Shin-ichi; Rieke, Reuben D.
Synthesis, 1984 , # 10 p. 842 - 844
反应条件
1: ammonium acetate / toluene; pyridine / 8 h / reflux 2: 70 percent / BNAH / Ru(bpy)32+ / methanol; pyridine / 1.5 h / Irradiation View Scheme
参考文献
Pac, Chyongjin; Miyauchi, Yoji; Ishitani, Osamu; Ihama, Mikio; Yasuda, Masahide; Sakurai, Hiroshi
Journal of Organic Chemistry, 1984 , vol. 49, # 1 p. 26 - 34
反应条件
[Ru(II)(2,2’-bipyridine)3]Cl2; NSC26899 in pyridine; methanol Irradiation; Yield given;
参考文献
Pac,C.; Ihama,M.; Yasuda,M.
Journal of the American Chemical Society, 1981 , vol. 103, p. 6495
反应条件
[Ru(II)(2,2’-bipyridine)3]Cl2; NSC26899 in pyridine; methanol Irradiation; Yield given;
参考文献
Pac,C.; Ihama,M.; Yasuda,M.
Journal of the American Chemical Society, 1981 , vol. 103, p. 6495
