1-苯基-1-己炔-3-醇合成路线 （共 21 条）
反应条件
zinc oxide T=120°C; 9 h; Neat (no solvent);
参考文献
Hosseini-Sarvari, Mona; Mardaneh, Zahra
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 12 p. 4297 - 4303
反应条件
indium in dichloromethane 0.4 h; Heating;
参考文献
Auge, Jacques; Lubin-Germain, Nadege; Seghrouchni, Latifa
Tetrahedron Letters, 2002 , vol. 43, # 30 p. 5255 - 5256
反应条件
1: (E/Z)-1-Fluoro-2-phenylethylene With lithium diisopropyl amide in tetrahydrofuran; hexane T=0°C; Metallation; 0.5 h; 2: butyraldehyde in tetrahydrofuran; hexane T=0 - 20°C; Substitution; Dehydrofluorination; 2.5 h;
参考文献
Kataoka, Kentaro; Tsuboi, Sadao
Synthesis, 2000 , # 3 p. 452 - 456
反应条件
indium tribromide; triethylamine in diethyl ether T=20°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 44, # 22 p. 4171 - 4174
反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane T=-30°C; 0.5 h; 2: Lithium enolate of the acetaldehyde; butyraldehyde in tetrahydrofuran; hexane T=-70 - -40°C; optical yield given as percent de;
参考文献
Liu, Jie; An, Yan; Wang, Ya-Hui; Jiang, Hai-Ying; Zhang, Yu-Xin; Chen, Zili
Chemistry - A European Journal, 2008 , vol. 14, # 30 p. 9131 - 9134
反应条件
1: 38 percent / KF / dimethylformamide / 15 h / 60 °C 2: 50 percent / HCl / H2O; ethanol / Ambient temperature View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 67, # 3 p. 412 - 416
反应条件
1: iodine; magnesium / tetrahydrofuran / 55 °C 2: tetrahydrofuran / 2 h / 55 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 17, # 25 p. 6918 - 6921
反应条件
diethyl ether T=-15°C;
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 35, p. 1177
反应条件
in tetrahydrofuran T=55°C; 2 h;
参考文献
Chemistry - A European Journal, , vol. 17, # 25 p. 6918 - 6921
反应条件
in tetrahydrofuran Addition; Alkynylation;
参考文献
Synlett, , # 9 p. 1330 - 1332
