1,3-二苯基-2-丙炔-1-醇合成路线 （共 82 条）
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran Phenylation; Sonogashira coupling; Heating;
参考文献
Angewandte Chemie - International Edition, , vol. 39, # 7 p. 1253 - 1256
反应条件
1: 2-phenylethynylmagnesium bromide in tetrahydrofuran; [TDTHP][Deca] T=-78 - 20°C; 2: benzaldehyde in [TDTHP][Deca]; toluene 16 h; 3: With water in [TDTHP][Deca]; toluene
参考文献
WO2006/7703 A1, ;
Page/Page column 28 ;
反应条件
buta-1,3-diene; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=25°C; Addition;
参考文献
Angewandte Chemie - International Edition, , vol. 38, # 22 p. 3386 - 3388
反应条件
diethylzinc; Ti(2,3-dihydro-2,2-dimethyl-7-benzofuran-O)4 in hexane; toluene T=25°C; 24 h; Product distribution; Further Variations:Temperatures;
参考文献
Dalton Transactions, , # 19 p. 2620 - 2626
反应条件
PhONn-Bu4 in tetrahydrofuran T=-78°C; 1 h;
参考文献
Chemistry Letters, , vol. 35, # 9 p. 1002 - 1003
反应条件
Chromium (III) chloride; lithium aluminium tetrahydride in N,N-dimethyl-formamide T=25°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 26, # 45 p. 5585 - 5588
反应条件
1: With 4-bromooctafluorobutanetriethoxysilane; diethylzinc; N,N-dimethyl-N'-(4-tert-butylphenyl)formamidine in tetrahydrofuran; hexane T=20 - 60°C; Inert atmosphere; 2: With sodium hydroxide in tetrahydrofuran; hexane; water T=0°C; 1 h;
参考文献
European Journal of Organic Chemistry, , # 25 p. 4893 - 4901
反应条件
1: benzoic acid ethyl ester With LDBBA in tetrahydrofuran; hexane T=0°C; 3 h; 2: lithium phenylacetylide in tetrahydrofuran; hexane T=20°C; 3 h;
参考文献
Chemical Communications, , vol. 47, # 11 p. 3281 - 3283
反应条件
niobium pentachloride in acetonitrile T=0 - 20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 50, # 30 p. 4318 - 4320
反应条件
phenyl-magnesium chloride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 6 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 67, # 1-4 p. 103 - 106
