2-甲酰基噁唑-4-羧酸乙酯合成路线 （共 3 条）
反应条件
ruthenium trichloride; sodium periodate; silica gel in dichloromethane T=20°C;
参考文献
Hartung, Ingo V.; Eggert, Ulrike; Haustedt, Lars Ole; Niess, Barbara; Schaefer, Peter M.; Hoffmann, H. Martin R.
Synthesis, 2003 , # 12 p. 1844 - 1850
反应条件
lead(IV) acetate; potassium carbonate in methanol T=0°C;
参考文献
Panek, James S.; Beresis, Richard T.
Journal of Organic Chemistry, 1996 , vol. 61, # 19 p. 6496 - 6497
反应条件
1: 1) NaHCO3, 2) TFAA / 1) THF, reflux, 23 h, 2) THF, 0 deg C 2: 85 percent / OsO4, Me3NO, H2O / acetone 3: 84 percent / Pb(OAc)4, K2CO3 / methanol / 0 °C View Scheme
参考文献
Actelion Pharmaceuticals Ltd.
Patent: US2012/115916 A1, 2012 ;
