3-甲基丙烯酰氧丙基戊二甲基二硅烷合成路线 (共 4 条)
反应条件
dihydrogen hexachloroplatinate; (10H)-phenothiazine in tetrahydrofuran T=90 - 95°C; 1.5 h;
参考文献
Efimov, Yu. T.; Tandura, T. A.; Kopylov, V. M.; Androsenko, S. I.; Shkol'nik, M. I.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 10 p. 2244 - 2253,2083 - 2091
反应条件
1: 72 percent / 0.05 N H2PtCl6, phenothiazine / tetrahydrofuran / 0.5 h / 80 °C 2: 95 percent / 5percent aq. hydrochloric acid / toluene / 0.5 h / 40 °C 3: cellular KU-23 sulfocation-exchange resin / Heating View Scheme
参考文献
Efimov, Yu. T.; Tandura, T. A.; Kopylov, V. M.; Androsenko, S. I.; Shkol'nik, M. I.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 10 p. 2244 - 2253,2083 - 2091
反应条件
1: 95 percent / 5percent aq. hydrochloric acid / toluene / 0.5 h / 40 °C 2: cellular KU-23 sulfocation-exchange resin / Heating View Scheme
参考文献
Efimov, Yu. T.; Tandura, T. A.; Kopylov, V. M.; Androsenko, S. I.; Shkol'nik, M. I.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 10 p. 2244 - 2253,2083 - 2091
反应条件
cellular KU-23 sulfocation-exchange resin Heating;
参考文献
Efimov, Yu. T.; Tandura, T. A.; Kopylov, V. M.; Androsenko, S. I.; Shkol'nik, M. I.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 10 p. 2244 - 2253,2083 - 2091