(3-碘丙基)(三甲基)硅烷合成路线 （共 9 条）
参考文献
Merrell Pharmaceuticals Inc.
Patent: US5536732 A1, 1996 ;
Title/Abstract Full Text Show Details
Merrell Dow Pharmaceuticals, Inc.
Patent: US5252587 A1, 1993 ;
反应条件
sodium iodide in acetone 18 h; Heating;
参考文献
Lee, Yean Jang; Ling, Rong; Mariano, Patrick S.; Yoon, Ung Chan; Kim, Dong Uk; Oh, Sun Wha
Journal of Organic Chemistry, 1996 , vol. 61, # 10 p. 3304 - 3314
反应条件
1: 100 percent / triethylamine / diethyl ether / 18 h / 25 °C 2: 99 percent / NaI / acetone / 18 h / Heating View Scheme
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
sodium iodide in acetone
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
1: LDA-HMPA / tetrahydrofuran
2: LiI, collidine / dimethylformamide / 140 °C
View Scheme
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
反应条件
potassium hydroxide; 18-crown-6 ether in benzene
6 h; Heating;
参考文献
Lukevics, Edmunds; Arsenyan, Pavel; Shestakova, Irina; Domracheva, Ilona; Nesterova, Alena; Pudova, Olga
European Journal of Medicinal Chemistry, 2001 , vol. 36, # 6 p. 507 - 515
