1-烯丙基-3-(三氟甲基)苯合成路线 （共 13 条）
反应条件
bromobenzene; zinc dibromide; zinc; acetic acid; cobalt(II) dibromide in acetonitrile T=20°C; 3 h;
参考文献
Organic Letters, , vol. 5, # 7 p. 1043 - 1045
反应条件
pyridine; tetrabutyl ammonium fluoride; cobalt(II) dibromide T=50°C; Electrolysis;
参考文献
Gomes, Paulo; Gosmini, Corinne; Perichon, Jacques
Journal of Organic Chemistry, 2003 , vol. 68, # 3 p. 1142 - 1145
反应条件
bis(1,5-cyclooctadiene)nickel (0); triethylsilyl trifluoromethanesulphonate; triethylamine; diphenylcyclohexyl phosphine in toluene T=20°C; Heck type reaction; P=760.051 Torr; 2 h;
参考文献
Matsubara, Ryosuke; Gutierrez, Alicia C.; Jamison, Timothy F.
Journal of the American Chemical Society, 2011 , vol. 133, # 47 p. 19020 - 19023
反应条件
magnesium in diethyl ether 1.) 30 min, room t.; 2.) reflux, 2 h;
参考文献
Goument, B.; Duhamel, L.; Mauge, R.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 459 - 466
反应条件
in acetonitrile T=-20°C; 4 h;
参考文献
Goument, B.; Duhamel, L.; Mauge, R.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 450 - 458
反应条件
1: 90 percent / 1.) magnesium, iodine; 2.) CuBr / diethyl ether / 1.) 2.5 h, 34-36 degC; 2.) -30 degC, 5 min, allowed to warm to 0 degC over 1 h, 3 h, 0 degC 2: thionylchloride, pyridine / 7.5 h / Heating View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 130, p. 450 - 458
参考文献
Journal of the American Chemical Society, , vol. 86, p. 233 - 238
参考文献
Goument, B.; Duhamel, L.; Mauge, R.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 450 - 458
反应条件
pyridine; thionyl chloride 7.5 h; Heating; Yield given. Yields of byproduct given;
参考文献
Bulletin de la Societe Chimique de France, , vol. 130, p. 450 - 458
参考文献
Journal of Organometallic Chemistry, , vol. 96, p. 225 - 235
