反应条件
1: 82 percent / conc. HCl
2: 1.) n-BuLi / 1.) THF, hexane, RT, 2 h, 2.) THF, RT, overnight
3: HCl / CHCl3 / 2 h / Ambient temperature
4: 85 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating
5: 84 percent / conc, HCl / CHCl3 / Ambient temperature
6: 91 percent / H2 / 10percent Pd/C / ethyl acetate / 982.6 Torr
View Scheme
参考文献
Holland; Qi; Manoharan
Canadian Journal of Chemistry, 1995 , vol. 73, # 9 p. 1399 - 1405
