2-氨基-5-氯二苯酮肟合成路线 （共 12 条）
反应条件
hydroxylamine hydrochloride in ethanol 10 h; Heating;
参考文献
Archiv der Pharmazie, , vol. 327, # 2 p. 77 - 84
反应条件
in acetic acid T=50°C; 0.166667 h;
参考文献
Lessel
Archiv der Pharmazie, 1994 , vol. 327, # 2 p. 77 - 84
参考文献
ASTON UNIVERSITY
Patent: WO2004/106310 A1, 2004 ;
Location in patent: Page 27 ;
WO 2004/106310 A1
反应条件
1: 94 percent / NaOH / diethyl ether; H2O / 3 h / 20 °C 2: 59.8 percent / aq. NaOH / ethanol / 20 °C / pH 12 - 14 View Scheme
参考文献
Offel, Michael; Lattmann, Pornthip; Singh, Harjit; Billington; Bunprakob, Yodchai; Sattayasai, Jintana; Lattmann, Eric
Archiv der Pharmazie, 2006 , vol. 339, # 4 p. 163 - 173
反应条件
1: 74 percent / acetic acid / 0.17 h / 50 °C
2: 96 percent / NH3 / methanol / 72 h / Ambient temperature
View Scheme
参考文献
Lessel
Archiv der Pharmazie, 1994 , vol. 327, # 2 p. 77 - 84
反应条件
1: 94.6 percent / Zn, CH3COONH4 / aq. NH3; ethanol / 3 h / Heating
2: 93 percent / glacial acetic acid / ethanol / 3 h / Heating
View Scheme
参考文献
Kempter, G.; Ehrlichmann, W.; Plesse, M.; Lehm, H.-U.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 5 p. 832 - 840
反应条件
1: 94.6 percent / Zn, CH3COONH4 / aq. NH3; ethanol / 3 h / Heating
2: 98 percent / glacial acetic acid / ethanol / 3 h / Heating
View Scheme
参考文献
Kempter, G.; Ehrlichmann, W.; Plesse, M.; Lehm, H.-U.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 5 p. 832 - 840
反应条件
1: 94.6 percent / Zn, CH3COONH4 / aq. NH3; ethanol / 3 h / Heating
2: 89 percent / glacial acetic acid / ethanol / 3 h / Heating
View Scheme
参考文献
Kempter, G.; Ehrlichmann, W.; Plesse, M.; Lehm, H.-U.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 5 p. 832 - 840
反应条件
1: 94.6 percent / Zn, CH3COONH4 / aq. NH3; ethanol / 3 h / Heating
2: 55 percent / xylene / 3 h / Heating
View Scheme
参考文献
Kempter, G.; Ehrlichmann, W.; Plesse, M.; Lehm, H.-U.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 5 p. 832 - 840
反应条件
1: 94.6 percent / Zn, CH3COONH4 / aq. NH3; ethanol / 3 h / Heating
2: 90 percent / xylene / 3 h / Heating
View Scheme
参考文献
Kempter, G.; Ehrlichmann, W.; Plesse, M.; Lehm, H.-U.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 5 p. 832 - 840
