2-甲氧基-4,5-二甲基苯胺合成路线 （共 9 条）
反应条件
in tetrahydrofuran; ethanol
参考文献
Samjin Pharmaceutical Co., Ltd.
Patent: US6028195 A1, 2000 ;
参考文献
Woolley; Pringle
Journal of Biological Chemistry, 1952 , vol. 194, p. 729,734
反应条件
palladium on activated charcoal; ethanol Hydrogenation;
参考文献
Matsukawa; Matsuno; Shirakawa
Yakugaku Zasshi, 1943 , vol. 63, p. 1,4
Chem.Abstr., 1950 , p. 7255
反应条件
1: aqueous formaldehyde; concentrated aqueous HCl / Einleiten von HCl 2: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Matsukawa; Matsuno; Shirakawa
Yakugaku Zasshi, 1943 , vol. 63, p. 1,4
Chem.Abstr., 1950 , p. 7255
反应条件
1: acetic acid; concentrated aqueous HNO3 2: Raney nickel; ethanol View Scheme
参考文献
Carruthers; Douglas
Journal of the Chemical Society, 1959 , p. 2813,2820
反应条件
hydrogenchloride T=145°C;
参考文献
Matsukawa; Matsuno; Shirakawa
Yakugaku Zasshi, 1943 , vol. 63, p. 1,4
Chem.Abstr., 1950 , p. 7255
反应条件
sulfuric acid; copper(II) sulfate
Diazotization;
参考文献
Tomita
Yakugaku Zasshi, 1936 , vol. 56, p. 814,822; dtsch. Ref. S. 142, 144
Chem.Abstr., 1938 , p. 8426
反应条件
sulfuric acid; sodium nitrite
Diazotization.Erwaermen der erhaltenen Diazoniumsalz-Loesung mit KI auf dem Dampfbad;
参考文献
Carruthers; Douglas
Journal of the Chemical Society, 1959 , p. 2813,2820
Full Text Show Details
Grewe
Chemische Berichte, 1938 , vol. 71, p. 907,910
反应条件
1: aqueous H2SO4; NaNO2 / Diazotization.Erwaermen der erhaltenen Diazoniumsalz-Loesung mit KI auf dem Dampfbad
2: copper-powder
3: aqueous HI; acetic acid
View Scheme
参考文献
Carruthers; Douglas
Journal of the Chemical Society, 1959 , p. 2813,2820
