3-烯丙氧基-4-甲氧基苯甲醛合成路线 （共 8 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=60°C;
参考文献
De Koning, Charles B.; Michael, Joseph P.; Rousseau, Amanda L.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 5 p. 787 - 797
反应条件
1: 4-hydroxy-3-(2-propenyloxy)benzaldehyde With sodium hydride in N,N-dimethyl-formamide T=20°C; 0.0833333 h; 2: methyl iodide in N,N-dimethyl-formamide T=20°C; 3.5 h; Further stages.;
参考文献
Hayashida, Maiko; Ishizaki, Miyuki; Hara, Hiroshi
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 9 p. 1299 - 1303
反应条件
iodine in dimethyl sulfoxide T=130°C; 0.5 h;
参考文献
Nawghare; Sakate; Lokhande
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 2 p. 291 - 302
反应条件
1: 95 percent / decahydronaphthalene / 5 h / 180 °C
2: K2CO3 / acetone / 8 h / Heating
View Scheme
参考文献
Huang, Keng-Shiang; Wang, Eng-Chi
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 2 p. 383 - 391
反应条件
1.1: K2CO3 / acetone
2.1: potassium tert-butoxide / tetrahydrofuran / 0.17 h
2.2: 80 percent / tetrahydrofuran
View Scheme
参考文献
Huang, Keng-Shiang; Wang, Eng-Chi
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 2 p. 383 - 391
反应条件
1: 92 percent / 3 h / 180 °C
2: K2CO3 / acetone / 8 h / Heating
3: H2O2; H(1+) / methanol / 1.5 h / 20 °C
View Scheme
参考文献
Wang, Eng-Chi; Hsu, Ming-Kun; Lin, Yu-Li; Huang, Keng-Shiang
Heterocycles, 2002 , vol. 57, # 11 p. 1997 - 2010
反应条件
1: 95 percent / decahydronaphthalene / 5 h / 180 °C
2: 88 percent / K2CO3 / acetone / 8 h / Heating
3: 96 percent / tetrahydrofuran / 2 h / 20 °C
4: 86 percent / [Ph-CH=RuCl2(PCy3)2] / CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
Huang, Keng-Shiang; Wang, Eng-Chi
Tetrahedron Letters, 2001 , vol. 42, # 35 p. 6155 - 6157
反应条件
1: microwave irradiation
2: 93 percent / K2CO3 / acetone / 2 h / 60 °C
3: 54 percent / [RuClH(CO)(PPh3)3] / CH2Cl2 / 14 h / 65 °C
4: 50 percent / ((Mes)2C3H5N2)Cl2Ru=CHPh / toluene / 3 h / 90 °C
View Scheme
参考文献
Van Otterlo, Willem A.L.; Morgans, Garreth L.; Madeley, Lee G.; Kuzvidza, Samuel; Moleele, Simon S.; Thornton, Natalie; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 32 p. 7746 - 7755
