2-重氮基-5,5-二甲基-1,3-环己二酮合成路线 （共 26 条）
反应条件
4-(N,N-dimethlyamino)pyridine; [bmim]Br; Methanesulfonyl azide T=25°C; 1 h;
参考文献
Ramachary, Dhevalapally B.; Narayana, Vidadala V.; Ramakumar, Kinthada
Tetrahedron Letters, 2008 , vol. 49, # 17 p. 2704 - 2709
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide T=55°C; 120 h;
参考文献
Benati, Luisa; Montevecchi, P. Carlo; Spagnolo, Piero
Gazzetta Chimica Italiana, 1992 , vol. 122, # 5-7 p. 249 - 251
反应条件
in dichloromethane 4 h; Heating;
参考文献
Kokel, Bruno; Viehe, Heinz Guenter
Angewandte Chemie, 1980 , vol. 92, # 9 p. 754 - 755
参考文献
Dieckmann
Chemische Berichte, 1902 , vol. 35, p. 3210
反应条件
dirhodium tetraacetate; dichloromethane; 3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide T=0 - 20°C;
参考文献
Schulze; Nikolaev; Hennig; Rodina; Sieler
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 5 p. 740 - 746
反应条件
dirhodium tetraacetate T=18 - 20°C; 2 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 42, # 11 p. 1741 - 1744
反应条件
(i) (irradiation), Me2S, (ii) H2O; Multistep reaction;
参考文献
Nikolaev,V.A. et al.
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 1433 - 1441,1338 - 1346
反应条件
in acetonitrile 2 h; Irradiation;
参考文献
Cossy, J.; Belotti, D.; Thellend, A.; Pete, J. P.
Synthesis, 1988 , # 9 p. 720 - 721
Title/Abstract Full Text Show Details
Cossy, Janine; Belotti, Damien; Bouzide, Abderahim; Thellend, Annie
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 723 - 729
反应条件
1,2-dichloro-ethane; dirhodium tetraacetate
T=20°C; 10 h;
参考文献
Lee, Yong Rok; Cho, Bang Sub; Kwon, Hyuk Jin
Tetrahedron, 2003 , vol. 59, # 47 p. 9333 - 9347
反应条件
fluorine in monofluoro-trichloromethane
参考文献
Patrick, Timothy B.; Scheibel, Jeffrey J.; Cantrell, Gary L.
Journal of Organic Chemistry, 1981 , vol. 46, # 19 p. 3917 - 3918
