1: With n-butyllithium in diethyl ether T=-70°C; 1 h; 2: With tellurium in diethyl ether T=-70 - 25°C; 1.5 h; 3: With iodine in diethyl ether T=25°C; 0.25 h;
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Klapoetke, Thomas M.; Krumm, Burkhard; Mayer, Peter; Polborn, Kurt; Ruscitti, Oliver P.
Journal of Fluorine Chemistry, 2001 , vol. 112, # 2 p. 207 - 212
Deacon, G. B.; Parrott, J. C.
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Gmelin Handbook: F: PerFHalOrg.2, 3, page 212 - 213