螺[吲哚啉-3,4’-哌啶]-1’-羧酸叔丁酯合成路线 （共 8 条）
反应条件
triethylamine in dichloromethane T=20°C; 2 h;
参考文献
Tetrahedron, , vol. 60, # 22 p. 4875 - 4878
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=100°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 37, # 30 p. 5233 - 5234
反应条件
1: 95 percent / LiAlH4 / ethanol; various solvent(s) / 72 h / Heating 2: 90 percent / Et3N / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 22 p. 4875 - 4878
反应条件
1: 17 g / aq. HCl / dioxane / 0.5 h / Heating 2: 95 percent / LiAlH4 / ethanol; various solvent(s) / 72 h / Heating 3: 90 percent / Et3N / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 22 p. 4875 - 4878
反应条件
1: 52 percent / K2CO3 / ethanol / 80 °C 2: 59 percent / Bu3SnH, AIBN / benzene / 12 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 30 p. 5233 - 5234
反应条件
1: 52 percent / 5percent SeO2/SiO2, t-BuOOH / Ambient temperature 2: 98 percent / thionyl chloride, 2,6-lutidine / toluene / 2 h / 35 °C 3: 52 percent / K2CO3 / ethanol / 80 °C 4: 59 percent / Bu3SnH, AIBN / benzene / 12 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 30 p. 5233 - 5234
反应条件
1: 98 percent / thionyl chloride, 2,6-lutidine / toluene / 2 h / 35 °C 2: 52 percent / K2CO3 / ethanol / 80 °C 3: 59 percent / Bu3SnH, AIBN / benzene / 12 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 30 p. 5233 - 5234
反应条件
1: 52 percent / K2CO3 / ethanol / 80 °C 2: 59 percent / Bu3SnH, AIBN / benzene / 12 h / 100 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 30 p. 5233 - 5234
