2,5-二溴对苯二甲酸二甲酯合成路线 （共 7 条）
反应条件
thionyl chloride 5 h; Reflux;
参考文献
Pham, Van Chung; Huh, Geun; Kim, Jungahn; Choo, Dong Joon; Lee, Jae Yeol
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 5 p. 1781 - 1783
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane; N,N-dimethyl-formamide T=20°C; 12 h; Inert atmosphere;
参考文献
Van Humbeck, Jeffrey F.; McDonald, Thomas M.; Jing, Xiaofei; Wiers, Brian M.; Zhu, Guangshan; Long, Jeffrey R.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2432 - 2440
反应条件
1: KMnO4; pyridine 2: H2SO4 View Scheme
参考文献
Macromolecules, , vol. 37, # 21 p. 7945 - 7954
反应条件
1: oxalyl dichloride / benzene; N,N-dimethyl-formamide / 2.5 h / |Inert atmosphere; |Reflux 2: pyridine; 4-(N,N-dimethlyamino)pyridine / N,N-dimethyl-formamide; dichloromethane / 12 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 136, # 6 p. 2432 - 2440
反应条件
(i) aq. KMnO4, (ii) /BRN= 1098229/, H2SO4; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 91, # 13 p. 3527 - 3533
参考文献
Bulletin de la Societe Chimique de France, , p. 1418,1420
反应条件
hydrogenchloride; iron(III) chloride; N,N-dimethyl-formamide
参考文献
Lawton; McRitchie
Journal of Organic Chemistry, 1959 , vol. 24, p. 26
