2,3-二苯基-1-二氢茚酮合成路线 (共 142 条)
反应条件
C70H44Cl2F64N2O6Pd2; tetrabutylammomium bromide; sodium carbonate in water T=170°C; 1 h; Microwave irradiationGreen chemistry; Reagent/catalyst; regioselective reaction;
参考文献
Ang, Wei Jie; Tai, Chih-Hsuan; Lo, Lee-Chiang; Lam, Yulin
RSC Advances, 2014 , vol. 4, # 10 p. 4921 - 4929
反应条件
[Rh(pentamethylcyclopentadienyl)(MeCN)3](SbF6)2; 2,2,2-trimethylacetic acid in 1,2-dichloro-ethane T=80°C; 15 h; Schlenk techniqueInert atmosphereSealed tube; Reagent/catalystSolvent;
参考文献
Qi, Zisong; Wang, Mei; Li, Xingwei
Organic Letters, 2013 , vol. 15, # 21 p. 5440 - 5443
反应条件
C70H44Cl2F64N2O6Pd2; tetrabutylammomium bromide; sodium carbonate in water T=150°C; 0.383333 h; Microwave irradiationGreen chemistry; regioselective reaction;
参考文献
Ang, Wei Jie; Tai, Chih-Hsuan; Lo, Lee-Chiang; Lam, Yulin
RSC Advances, 2014 , vol. 4, # 10 p. 4921 - 4929
反应条件
zinc; CoI2(dppe) in acetonitrile T=80°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 14 p. 4781 - 4787
反应条件
Pd(O2CCF3)2(dppe) in methanol T=80°C; 16 h;
参考文献
Tsukamoto, Hirokazu; Kondo, Yoshinori
Organic Letters, 2007 , vol. 9, # 21 p. 4227 - 4230
反应条件
[Rh(pentamethylcyclopentadienyl)(MeCN)3](SbF6)2; copper diacetate in decalin T=120°C; 12 h; Inert atmosphere;
参考文献
Li, Bi-Jie; Wang, Hao-Yuan; Zhu, Qi-Lei; Shi, Zhang-Jie
Angewandte Chemie - International Edition, 2012 , vol. 51, # 16 p. 3948 - 3952
反应条件
ammonium cerium(IV) nitrate in anhydrous butyl ether T=90°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 36, # 45 p. 8159 - 8162
反应条件
sulfuric acid; acetic acid
参考文献
Chemische Berichte, , vol. 54, p. 2343
反应条件
silver hexafluoroantimonate; [Rh(pentamethylcyclopentadienyl)(MeCN)3](SbF6)2; acetic acid hydrazide; silver carbonate in acetic acid T=120°C; 14 h; Inert atmosphereSealed tube; Catalytic behaviorMechanism; Reagent/catalystSolvent;
参考文献
Chen, Shuyou; Yu, Jintao; Jiang, Yan; Chen, Fan; Cheng, Jiang
Organic Letters, 2013 , vol. 15, # 18 p. 4754 - 4757
反应条件
methyl trifluoromethanesulfonate in 1,2-dichloro-ethane T=160°C; 12 h; Inert atmosphereSealed tube;
参考文献
Yan, Xiaoyu; Zou, Song; Zhao, Peng; Xi, Chanjuan
Chemical Communications, 2014 , vol. 50, # 21 p. 2775 - 2777