2,3-二苯基-1-二氢茚酮合成路线 (共 142 条)
反应条件
sodium carbonate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,4-dioxane; water T=80°C; P=760.051 Torr; 20 h;
参考文献
Harada, Yasuyuki; Nakanishi, Jun; Fujihara, Hirokazu; Tobisu, Mamoru; Fukumoto, Yoshiya; Chatani, Naoto
Journal of the American Chemical Society, 2007 , vol. 129, # 17 p. 5766 - 5771
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane; water T=70°C; Suzuki-Miyaura reaction; 6 h; Inert atmosphere;
参考文献
Khera, Rasheed Ahmad; Hussain, Munawar; Hung, Nguyen Thai; Eleya, Nadi; Feist, Holger; Villinger, Alexander; Langer, Peter
Helvetica Chimica Acta, 2012 , vol. 95, # 3 p. 469 - 482
反应条件
1: 2-Iodobenzaldehyde With tert-butylamine in N,N-dimethyl-formamide Inert atmosphere; 2: diphenyl acetylene With [Pd(.eta.(5)-C5H5)Fe(.eta.(5)-C5H3-C(CH3)=N-C6H4-4-CH3)Cl(P(C6H5)3)]; sodium carbonate; lithium chloride in N,N-dimethyl-formamide T=100°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 67, # 16 p. 2969 - 2973
反应条件
1: ortho-bromobenzaldehyde With tert-butylamine in N,N-dimethyl-formamide Inert atmosphere; 2: diphenyl acetylene With [Pd(.eta.(5)-C5H5)Fe(.eta.(5)-C5H3-C(CH3)=N-C6H4-4-CH3)Cl(P(C6H5)3)]; sodium carbonate; lithium chloride in N,N-dimethyl-formamide T=100°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 67, # 16 p. 2969 - 2973
反应条件
zinc; tetracarbonylbis(μ-chloro)dirhodium(I) in ethanol T=120°C; 3.5 h;
参考文献
Wender, Paul A.; Paxton, Thomas J.; Williams, Travis J.
Journal of the American Chemical Society, 2006 , vol. 128, # 46 p. 14814 - 14815
反应条件
C70H44Cl2F64N2O6Pd2; tetrabutylammomium bromide; sodium carbonate in water T=150°C; 0.333333 h; Microwave irradiationGreen chemistry; Reagent/catalyst; regioselective reaction;
参考文献
Ang, Wei Jie; Tai, Chih-Hsuan; Lo, Lee-Chiang; Lam, Yulin
RSC Advances, 2014 , vol. 4, # 10 p. 4921 - 4929
反应条件
water; triethylamine; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=130°C; 24 h;
参考文献
Pletnev, Alexandre A.; Tian, Qingping; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9276 - 9287
反应条件
water; [Rh(OH)(cycloocta-1,5-diene)]2 in 1,4-dioxane T=100°C; 48 h;
参考文献
Miura, Tomoya; Murakami, Masahiro
Organic Letters, 2005 , vol. 7, # 15 p. 3339 - 3341
反应条件
water; iodine in tetrahydrofuran T=50°C; 24 h;
参考文献
Wang, Chengyu; Yang, Jingyu; Cheng, Xingcan; Li, Ende; Li, Yanzhong
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4402 - 4404
反应条件
1,10-phenanthroline; oxygen; copper diacetate in N,N-dimethyl-formamide T=60°C; P=760.051 Torr; 12 h; Schlenk technique;
参考文献
Zhao, Peng; Wang, Fen; Han, Keli; Li, Xingwei
Organic Letters, 2012 , vol. 14, # 21 p. 5506 - 5509,4