1,5-二叠氮-9-壬烯[5.5]十一烷合成路线 （共 5 条）
反应条件
phosphoric acid T=65°C; 6 h; Inert atmosphere;
参考文献
Wang, Jun; Cady, Sarah D.; Balannik, Victoria; Pinto, Lawrence H.; DeGrado, William F.; Hong, Mei
Journal of the American Chemical Society, 2009 , vol. 131, p. 8066 - 8076
反应条件
palladium 10 on activated carbon; hydrogen in methanol P=760.051 Torr;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 10 p. 2288 - 2294
反应条件
1: toluene-4-sulfonic acid / chloroform / |Inert atmosphere; |Reflux; |Molecular sieve 2: potassium hydroxide; water / ethanol / 20 h / |Reflux View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 8, p. 1700 - 1704
反应条件
water; potassium hydroxide in ethanol 20 h; Reflux;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 8, p. 1700 - 1704
反应条件
1: toluene-4-sulfonic acid / toluene / 135 - 140 °C / |Dean-Stark 2: hydrogen; palladium 10 on activated carbon / methanol / 760.05 Torr View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 10 p. 2288 - 2294
