反应条件
1: copper / dimethyl sulfoxide / 12 h / 60 °C / |Inert atmosphere 2: thionyl chloride / 0 - 20 °C / |Inert atmosphere 3: sodium hydroxide / methanol / 5 h / 20 °C / |Inert atmosphere 4: 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); silver nitrate / water; acetone / 1 h / 55 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Mizuta, Satoshi; Stenhagen, Ida S.R.; O'Duill, Miriam; Wolstenhulme, Jamie; Kirjavainen, Anna K.; Forsback, Sarita J.; Tredwell, Matthew; Sandford, Graham; Moore, Peter R.; Huiban, Mickael; Luthra, Sajinder K.; Passchier, Jan; Solin, Olof; Gouverneur, Veronique
Organic Letters, 2013 , vol. 15, # 11 p. 2648 - 2651
