1,3-二氯-1,1,3,3-四乙基二锡氧烷合成路线 （共 4 条）
反应条件
methanol in methanol; water byproducts: Cl(1-), (Sn(CH2CH3)2)3O2Cl2; MeOH:H2O = 90:10, pH 2.2; not isolated, detected by electrospray MS;
参考文献
Ghys, Laurent; Biesemans, Monique; Gielen, Marcel; Garoufis, Achilleas; Hadjiliadis, Nick; Willem, Rudolph; Martins, Jose C.
European Journal of Inorganic Chemistry, 2000 , # 3 p. 513 - 522
反应条件
ozone in tetrachloromethane passing of ozone (2-5 vol-percent on O2 stream) though soln. (20°C), pptn.;
参考文献
Tarunin, B. I.; Perepletchikov, K. L.; Aleksandrov, Yu. A.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 1861 - 1863
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 2298 - 2300
反应条件
sodium hydroxide in water byproducts: Cl(1-); addn. NaOH to pH 2.8; also in the presence of cytosine-5'-monophosphateat pH 2-5;; filtration; elem. anal.; NMR;
参考文献
Ghys, Laurent; Biesemans, Monique; Gielen, Marcel; Garoufis, Achilleas; Hadjiliadis, Nick; Willem, Rudolph; Martins, Jose C.
European Journal of Inorganic Chemistry, 2000 , # 3 p. 513 - 522
反应条件
ozone in hexane passing of ozone (2-5 vol-percent on O2 stream) though soln. (-78°C), pptn.; washing (-78°C);
参考文献
Tarunin, B. I.; Perepletchikov, K. L.; Aleksandrov, Yu. A.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 1861 - 1863
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 2298 - 2300
