三(三甲代甲硅烷基)亚磷酸盐合成路线 (共 38 条)
反应条件
in toluene Ambient temperature;
参考文献
Muller; Roth
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 501 - 502
反应条件
in toluene Ambient temperature;
参考文献
Muller; Roth
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 501 - 502
反应条件
trityl-glycidol T=130 - 150°C;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 107, # 1-4 p. 27 - 32
参考文献
Sekine,M.; Hata,T.
Journal of the Chemical Society, Chemical Communications, 1978 , p. 285 - 286
反应条件
T=20°C; Substitution; 4 h;
参考文献
Saakyan
Russian Journal of General Chemistry, 1999 , vol. 69, # 11 p. 1712 - 1716
反应条件
iodine in diethyl ether T=-40 - -30°C; 0.5 h;
参考文献
Michalski, Jan; Pakulski, Marek; Skowronska, Aleksandra
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 833 - 836
反应条件
Michaelis-Arbuzov reaction; 0.0166667 h; microwave irradiation;
参考文献
Kiddle, James J.; Gurley, Alison F.
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 160, p. 195 - 205
参考文献
D'yakov,V.M. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1972 , vol. 42, p. 1291 - 1295,1286 - 1289
参考文献
Sekine,M.; Hata,T.
Journal of the Chemical Society, Chemical Communications, 1978 , p. 285 - 286
反应条件
triethylamine
1.) room temperature, 1 h, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Sekine, Mitsuo; Futatsugi, Tetsuaki; Yamada, Kohji; Hata, Tsujiaki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 11 p. 2509 - 2514