triphenylphosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in benzene stirring under N2 at 100 or 80 °C for 10 h gave various yields;
phenyl-magnesium bromide in dichloromethane Ge compd. and equimol. amt. of SnCl4 reacted in CH2Cl2 at room temp. to give the SnCl3 compd.; SnCl3 compd. reacted in THF at - 78 °C with 5 mol. amts. of PhMgBr;
参考文献
Takeda, Takeshi; Tamada, Yoshitake; Yamaguchi, Jun-ichi; Fujiwara, Tooru
Nippon Kagaku Kaishi (Journal of the Chemical Society of Japan), 1994 , p. 301 - 306
