2-(甲氧基羰基)苯基异氰酸酯合成路线 （共 17 条）
反应条件
pyridine in dichloromethane T=20°C; 4 h;
参考文献
SPIROGEN LIMITED
Patent: WO2005/23814 A1, 2005 ;
Location in patent: Page/Page column 106 ;
反应条件
in dichloromethane; toluene T=0°C; 0.166667 h;
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 7 p. 1932 - 1935
参考文献
Lebedev; Lebedeva; Sheludyakov; Ovcharuk; Kovaleva; Ustinova
Russian Journal of General Chemistry, 2006 , vol. 76, # 7 p. 1069 - 1080
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran; dichloromethane T=0 - 20°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 24 p. 6723 - 6728
反应条件
sodium azide; chloroformic acid ethyl ester; triethylamine 1.) THF, 0 deg C, 1 h, 2.) THF, H2O, 1 h; Yield given. Multistep reaction;
参考文献
Heterocycles, , vol. 36, # 6 p. 1305 - 1314
反应条件
1: 97 percent / sulfuric acid / 0.5 h / Heating 2: 95 percent / toluene / 0 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 76, # 7 p. 1069 - 1080
反应条件
sodium hydroxide in 1,4-dioxane; water T=50°C; 4 h;
参考文献
Canonne, Persephone; Akssira, Mohamed; Dahdouh, Abdelaziz; Kasmi, Hicham; Boumzebra, Mohamed
Heterocycles, 1993 , vol. 36, # 6 p. 1305 - 1314
反应条件
1: tetrahydrofuran / 8 h / Ambient temperature 2: conc. H2SO4 / 3 h View Scheme
参考文献
Krantz; Spencer; Tam; Liak; Copp; Thomas; Rafferty
Journal of Medicinal Chemistry, 1990 , vol. 33, # 2 p. 464 - 479
反应条件
in tetrahydrofuran 8 h; Ambient temperature;
参考文献
Krantz; Spencer; Tam; Liak; Copp; Thomas; Rafferty
Journal of Medicinal Chemistry, 1990 , vol. 33, # 2 p. 464 - 479
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Hays, Sheryl J.; Caprathe, Bradley W.; Gilmore, John L.; Amin, Nilam; Emmerling, Mark R.; Michael, Walter; Nadimpalli, Ravi; Nath, Rathna; Raser, Kadee J.; Stafford, Daniel; Watson, Desiree; Wang, Kevin; Jaen, Juan C.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 7 p. 1060 - 1067
