3-氨基-6-溴吡嗪-2-甲酰胺合成路线 （共 4 条）
反应条件
bromine; acetic acid T=20 - 25°C; 0.333333 h;
参考文献
Duan, Chonggang; Jia, Jiong; Zhu, Rongxiu; Wang, Jianwu
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 4 p. 865 - 872
反应条件
1: ammonia / water; methanol / 24 h / 30 °C 2: sodium acetate; bromine; acetic acid / 2 h / 50 - 55 °C View Scheme
反应条件
1: sulfuric acid / 50 h / 25 - 30 °C 2: ammonia / water / 12 h / 20 °C 3: acetic acid; bromine / 0.33 h / 20 - 25 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 49, # 4 p. 865 - 872
反应条件
1: With hydrogen bromide; bromine in acetic acid T=-10°C; 0.75 h; 2: With sodium nitrite in water T=-10 - -5°C; 2.5 h;
参考文献
WIGERINCK, Piet Tom Bert Paul; ANDREWS, Martin James Inglis; De WEER, Marc Maurice Germain; SABOURAULT, Nicholas Luc; KLUGE, Stefan Christian
Patent: US2011/118269 A1, 2011 ;
Location in patent: Page/Page column 13-14 ;
