4-甲基-6-叔丁基香豆素合成路线 （共 8 条）
反应条件
trifluoroacetic acid; trifluoroacetic anhydride; palladium diacetate in dichloromethane T=20°C; Cyclization; hydroarylation; 2 h;
参考文献
Jia, Chengguo; Piao, Dongguo; Kitamura, Tsugio; Fujiwara, Yuzo
Journal of Organic Chemistry, 2000 , vol. 65, # 22 p. 7516 - 7522
反应条件
1: 80 percent / DCC; 4-dimethylaminopyridine / 20 °C 2: 90 percent / TFA / Pd(OAc)2 / CH2Cl2 / 0.5 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 22 p. 7516 - 7522
反应条件
sulfuric acid T=20°C; 24 h;
参考文献
Voss, Jrgen; Edler, Ronald; Adiwidjaja, Gunadi
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 8 p. 1893 - 1905
反应条件
sulfuric acid T=20°C; 24 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 182, # 8 p. 1893 - 1905
反应条件
1: 37 percent / NEt3 / CHCl3 / 7 h / Heating 2: 2.3 percent / aq. H2SO4 / 24 h / 20 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 182, # 8 p. 1893 - 1905
反应条件
sodium acetate T=160°C;
参考文献
Journal of the Indian Chemical Society, , vol. 29, p. 950,952
反应条件
sulfuric acid T=85°C; 1 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 182, # 8 p. 1893 - 1905
反应条件
1: AlCl3 2: sodium acetate / 160 °C View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 29, p. 950,952
