2-(三丁基锡烷基)苯乙酮合成路线 （共 21 条）
反应条件
acetophenone; lithium diisopropyl amide in tetrahydrofuran byproducts: LiCl; C6H5COCH3 treated with lithium diisopropylamide at 0°C in THF, Sn compd. added, reacted for 10 min; THF removed (vac.), C6D6 added, centrifuged, not isolated, detected by NMR;
参考文献
Yamamoto, Yoshinori; Maruyama, Kazuhiro
Journal of the American Chemical Society, 1982 , vol. 104, # 8 p. 2323 - 2325
反应条件
in chloroform-d1 room temp.; detected by 119Sn NMR;
参考文献
Pereyre et al.
Journal of Organometallic Chemistry, 1968 , vol. 11, p. 97
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Lutsenko et al.
Journal of Organometallic Chemistry, 1969 , vol. 17, p. P13
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Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.5.2, page 276 - 305
参考文献
Lesbre, M.; Buisson, R.
Bulletin de la Societe Chimique de France, 1957 , p. 1204 - 1206
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.5.2, page 276 - 305
反应条件
byproducts: CH3COCH3; equimolar amts. of educts; heating to 120°C/400 Torr for 40 h; mixt. of products in ratio of 22:78;
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.2, page 97 - 113
反应条件
at 120°C/400 Torr for 20 h; mixt. of products in ratio of 22:78;
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.2, page 97 - 113
反应条件
in dimethyl sulfoxide byproducts: ethylacetate; Ar; 75°C, 36 h; distn.;
参考文献
Kashin, A. N.; Tulchinsky, M. L.; Beletskaya, I. P.
Journal of Organometallic Chemistry, 1985 , vol. 292, p. 205 - 216
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.1, page 38 - 56
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.1, page 38 - 56
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.1, page 38 - 56
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.1, page 38 - 56
