乙酸1,4-二氧代-1,4-二氢萘-2-基酯合成路线 (共 17 条)
反应条件
1: 2-hydroxynaphthalene-1,4-dione With triethylamine in ethyl acetate T=5 - 10°C; 1 h; 2: acetic anhydride in ethyl acetate T=5 - 10°C; 4.5 h;
参考文献
Nardi, Antonio; Sada, Mara; Salvi, Annibale; Maiorana, Stefano
Patent: US2010/137644 A1, 2010 ;
Location in patent: Page/Page column 3-4 ;
反应条件
potassium carbonate in acetone T=20°C;
参考文献
Smith, Robert B.; Canton, Claire; Lawrence, Nathan S.; Livingstone, Callum; Davis, James
New Journal of Chemistry, 2006 , vol. 30, # 12 p. 1718 - 1724
反应条件
iron(II) diperchlorate; dihydrogen peroxide; acetic anhydride; acetonitrile T=30°C; 0.05 h; Further byproducts given;
参考文献
Kotani, Eiichi; Kobayashi. Shigeki; Ishii, Yoko; Tobinaga, Seisho
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4671 - 4679
反应条件
iron(II) diperchlorate; dihydrogen peroxide; acetonitrile T=30°C; 0.05 h; Further byproducts given;
参考文献
Kotani, Eiichi; Kobayashi. Shigeki; Ishii, Yoko; Tobinaga, Seisho
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4671 - 4679
反应条件
chromium(VI) oxide T=0°C;
参考文献
Cort,L.A.; Rodriguez,P.A.B.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 949 - 952
反应条件
lead(IV) acetate in acetic acid 0.00833333 h; Ambient temperature;
参考文献
Greenland, Harry; Pinhey, John T.; Sternhell, Sever
Australian Journal of Chemistry, 1986 , vol. 39, p. 2067 - 2074
反应条件
1: alcohol; hydrochloric acid 2: ice; sulfuric acid; dichromate / 0 °C 3: zinc chloride View Scheme
参考文献
Thiele; Winter
Justus Liebigs Annalen der Chemie, 1900 , vol. 311, p. 355
Chem. Zentralbl., 1901 , vol. 72, # II p. 70
反应条件
1: ice; sulfuric acid; dichromate / 0 °C 2: zinc chloride View Scheme
参考文献
Thiele; Winter
Justus Liebigs Annalen der Chemie, 1900 , vol. 311, p. 355
Chem. Zentralbl., 1901 , vol. 72, # II p. 70
反应条件
1: ZnCl2 / 50 - 60 °C 2: alcohol; hydrochloric acid 3: ice; sulfuric acid; dichromate / 0 °C 4: zinc chloride View Scheme
参考文献
Thiele; Winter
Justus Liebigs Annalen der Chemie, 1900 , vol. 311, p. 355
Chem. Zentralbl., 1901 , vol. 72, # II p. 70
反应条件
1: ZnCl2 / 50 - 60 °C 2: alcohol; hydrochloric acid 3: ice; sulfuric acid; dichromate / 0 °C 4: zinc chloride View Scheme
参考文献
Thiele; Winter
Justus Liebigs Annalen der Chemie, 1900 , vol. 311, p. 355
Chem. Zentralbl., 1901 , vol. 72, # II p. 70