乙基(二乙氧基磷酰)(二氟)乙酸酯合成路线 (共 2 条)
参考文献
Burton, Donald J.; Sprague, Lee G.; Pietrzyk, Donald J.; Edelmuth, Steven H.
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3437 - 3438
反应条件
Stage #1: With sodium hydride in tetrahydrofuran T=0 - 20°C; 2 h; Stage #2: With 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in tetrahydrofuran T=0 - 20°C; 4 h;
参考文献
Marma, Mong S.; Khawli, Leslie A.; Harutunian, Vahak; Kashemirov, Boris A.; McKenna, Charles E. Journal of Fluorine Chemistry, 2005 , vol. 126, # 11-12 p. 1467 - 1475