(4-亚甲基-5-己烯基)三苯基-鏻碘化物合成路线 （共 6 条）
反应条件
1: 63 percent / 1.) ozone, 2.) aq. NaBH4 / methanol / 1.) -78 deg C, 2.) RT, 2 h 2: 63 percent / (PhO)3PMeI 3: 77 percent View Scheme
参考文献
Stenstroem, Yngve; Skatteboel, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 2 p. 131 - 132
参考文献
Stenstroem, Yngve; Skatteboel, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 2 p. 131 - 132
反应条件
1: 63 percent / (PhO)3PMeI 2: 77 percent View Scheme
参考文献
Stenstroem, Yngve; Skatteboel, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 2 p. 131 - 132
反应条件
1: tetrahydrofuran / Ambient temperature View Scheme
参考文献
Baumann,M. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1626 - 1633
参考文献
Baumann,M. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1626 - 1633
反应条件
n-butyllithium
1.) THF, hexane, -20 deg C, 45 min, 2.) 4 h, RT; Yield given. Multistep reaction;
参考文献
Stenstroem, Yngve; Skatteboel, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 2 p. 131 - 132
