4-氯-2H-色烯-2-酮合成路线 （共 25 条）
反应条件
triethylamine; trichlorophosphate 1.5 h; Reflux;
参考文献
Zhang, Wenjuan; Li, Zhi; Zhou, Meng; Wu, Feng; Hou, Xueyan; Luo, Hao; Liu, Hao; Han, Xuan; Yan, Guoyi; Ding, Zhenyu; Li, Rui
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 3 p. 799 - 807
反应条件
1: With trichlorophosphate T=-10 - 60°C; 3 h; 2: With water T=0°C;
参考文献
Steinfuehrer, Thorsten; Hantschmann, Achim; Pietsch, Michael; Weissenfels, Manfred
Liebigs Annalen der Chemie, 1992 , # 1 p. 23 - 28
反应条件
1: N,N-dimethyl acetamide With trichlorophosphate in 1,2-dichloro-ethane T=20°C; Cooling with ice; 2: salicylic acid in 1,2-dichloro-ethane T=20 - 95°C; 24.3333 h; 3: With water; sodium acetate in 1,2-dichloro-ethane T=90°C; 1 h;
参考文献
Roma, Giorgio; Piras, Daniela; Di Braccio, Mario; Grossi, Giancarlo
Synthesis, 2010 , # 5 art. no. Z22309SS, p. 849 - 857
反应条件
trichlorophosphate T=80°C; 5 h;
参考文献
Ghosh, Tarun; Sur, Kumar Ranabir; Bandyopadhyay, Chandrakanta
Journal of Chemical Research, 2006 , # 10 p. 651 - 654
反应条件
zinc(II) chloride; trichlorophosphate T=70 - 80°C; 4 h;
参考文献
Shah; Desai; Trivedi
Pharmazie, 1983 , vol. 38, # 7 p. 439 - 441
反应条件
trichlorophosphate 1 h; Reflux;
参考文献
Patel, Divyesh; Kumari, Premlata; Patel, Navin B.
Medicinal Chemistry Research, 2013 , vol. 22, # 2 p. 726 - 744
参考文献
Justus Liebigs Annalen der Chemie, , vol. 367, p. 174
Justus Liebigs Annalen der Chemie, , vol. 368, p. 43
反应条件
methyllithium in diethyl ether T=-50°C; 2 h;
参考文献
Alberola, Angel; Calvo, Blanca; Ortega, Alfonso Gonzalez; Pedrosa, Rafael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 22 p. 3075 - 3080
反应条件
in tetrahydrofuran T=-50°C; 2 h;
参考文献
Alberola, Angel; Calvo, Blanca; Ortega, Alfonso Gonzalez; Pedrosa, Rafael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 22 p. 3075 - 3080
反应条件
in diethyl ether T=-50°C; 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 22 p. 3075 - 3080
