2-联苯基膦基-1-萘甲酸合成路线 （共 4 条）
反应条件
Ba(OH)2*8H2O in methanol Hydrolysis; 25 h; Heating;
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
1: 89 percent / pyridine / CH2Cl2 / 14 h / 0 °C 2: 95 percent / bis(benzonitrile)palladium dichloride / toluene / 26 h / Heating 3: 88 percent / barium hydroxide octahydrate / methanol / 25 h / Heating View Scheme
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
1: 95 percent / bis(benzonitrile)palladium dichloride / toluene / 26 h / Heating 2: 88 percent / barium hydroxide octahydrate / methanol / 25 h / Heating View Scheme
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine in dichloromethane T=-78 - 0°C; 17 h; Inert atmosphere;
参考文献
Trost, Barry M.; O'Boyle, Brendan M.
Organic Letters, 2008 , vol. 10, # 7 p. 1369 - 1372
