螺[5.5]十一烷-2-酮合成路线 (共 6 条)
反应条件
ammonia; lithium in diethyl ether T=-40°C; 2.5 h;
参考文献
Ruppert, John F.; White, James D.
Journal of the American Chemical Society, 1981 , vol. 103, # 7 p. 1808 - 1813
参考文献
de Jongh,H.A.P.; Wynberg,H.
Tetrahedron, 1964 , vol. 20, p. 2553 - 2573
反应条件
CuSPh in tetrahydrofuran 1.) -78 deg C to -15 deg C, 20 min, -15 deg C, 10 min, 2.) -15 deg C, 1 h;
参考文献
Wender, Paul A.; White, Alan W.
Journal of the American Chemical Society, 1988 , vol. 110, # 7 p. 2218 - 2223
反应条件
1: chloroform; phosphorus trichloride 2: zinc dust; glacial acetic acid View Scheme
参考文献
de Jongh,H.A.P.; Wynberg,H.
Tetrahedron, 1964 , vol. 20, p. 2553 - 2573
反应条件
N(Et)4ClO4; NH4Br; Ni(trans-lt;14gt;aneN4)(ClO4)2 in N,N-dimethyl-formamide electroreduction (divided cell, glassy-carbon plate electrode);
参考文献
Scheffold, Rolf; Dike, Meera; Dike, Sunneel; Herold, Thomas; Walder, Lorenz
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3642 - 3644
参考文献
Norris
Journal of the Chemical Society, 1926 , p. 249